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International Journal of Environment Science and Technology
Center for Environment and Energy Research and Studies (CEERS)
ISSN: 1735-1472 EISSN: 1735-1472
Vol. 11, No. 1, 2014, pp. 217-232
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Bioline Code: st14023
Full paper language: English
Document type: Research Article
Document available free of charge
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International Journal of Environment Science and Technology, Vol. 11, No. 1, 2014, pp. 217-232
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Characterization of PM2.5 by X-ray diffraction and scanning electron microscopy–energy dispersive spectrometer: its relation with different pollution sources
Satsangi, P. G. & Yadav, S.
Abstract
Atmospheric PM2.5 samples were collected by
using Mini-Vol TAS air sampler. Samples were characterized
directly on the collecting substrate using X-ray
diffraction and scanning electron microscopy–energy dispersive
spectrometer. From the analysis, it was found that
Si dominate over other elements which follows the trend as
Si>S>Zn>Cu>Na>Al>K>Ca>P>Fe>Mg
>Ti. Based on the measurements of a population of 840
particles, particle morphology was determined by quantitative
image analyzer and value of roundness (R) varies
from 0.23 to 1.0 (mean 0.75) which suggests that particles
vary in shape from nearly irregular to perfectly spherical
shape. The mineral particulate matter identified in the
atmosphere of Pune was made up of: silicates (52 %),
oxides (22 %), sulfates (8 %), phosphates (7 %), carbonates
(3 %) and others. A factorial analysis was carried out
to determine the main elements related to the emission
sources such as soil and building material erosion
(∼44.6 %); oil combustion (20.6 %) and fuel and biomass
burning (18.3 %). Besides these factors, soot particles are
abundantly present in all studied samples. Mineral particles
such as sulfates aggregated to soot could have produced
localized climatic effect in Pune. The emphasis of the
present study is to give insight and detailed analysis of
morphological and chemical composition of atmospheric
particles at discrete level.
Keywords
Elemental composition; Minerals; Particulate morphology; Soot
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